Advances in Carbohydrate Chemistry, Vol. 5 by Claude S. Hudson, etc.

By Claude S. Hudson, etc.

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Extra info for Advances in Carbohydrate Chemistry, Vol. 5

Example text

V. Synthetic Non-reducing Disnccharides . . . . . . . . . . . . . . . . 1. Synthetic Sucrose.. . . . . . . . . . . . . . . . . . . . . . a. Preparation of the Enzymatic Extract from Pseudomonas saccharophila . . . . . . . . . . . . b. Enzymatic Synthesis and Isolation of Synthetic Sucrose. . . . c. Properties of Synthetic Sucrose ................... 2. a-D-Glucopyranosyl-D-D-xyloketofuranoside.. .

70, 3955 (1948); H. Hauenstein and T. Reichatein, Helv. Chim. Ada, 92, 22 (1949). (66) M. L. Wolfrom and J. V. Karabinos, J . Am. Chem. , 68,724, 1455 (1946). (66) Personal communication from Dr. J. V. Karabinos. Subsequent work on the reduction of steroid acids by Spero, McIntosh and Levin (ref. 12) has shown that Raney nickel partially deactivated by acetone is particularly suitable for the desulfurization of thiol esters to aldehydes. DESULFURIZATION BY RANEY NICKEL 23 freshly prepared material ; almost simultaneous work by Jeger, Norymberski, Szpilfogel and Preloge7 showed that fresh Raney nickel readily carries the thiol ester over to the alcohol stage.

Chem. ,I S , 1602 (1937). D. A. Rosenfeld, N. K. Richtmyer and C. S. Hudson, J. Am. Chem. , (1948). 18 HEWITT 0. , AND NELSON K. RICHTMYER Two new anhydrides, 1,5-anhydro-4-(&~-galactopyranosyl)-~-glucitol (1,5-anhydrolactitol) (LIII) and 1,5-anhydro-4-(a-~-glucopyranosyl)-~glucitol (1,5-anhydromaltitol) (LV) have recently been synthesized66 through the reductive desulfurization of 2'-naphthyl l-thio-p-lactopyranoside (LII) and phenyl 1-thio-8-ma1t opyranoside heptaaceta te (LIV), respectively .

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